2-(Methoxycarbonyl)-6-methylaniline, 2-Amino-3-(methoxycarbonyl)toluene, Methyl 3-methylanthranilate
Methyl 2-Amino-3-Methylbenzoate
CAS: 22223-49-0
Molecular Formula: C9H11NO2
2-(Methoxycarbonyl)-6-methylaniline, 2-Amino-3-(methoxycarbonyl)toluene, Methyl 3-methylanthranilate - Names and Identifiers
2-(Methoxycarbonyl)-6-methylaniline, 2-Amino-3-(methoxycarbonyl)toluene, Methyl 3-methylanthranilate - Physico-chemical Properties
| Molecular Formula | C9H11NO2 |
| Molar Mass | 165.19 |
| Density | 1.132±0.06 g/cm3(Predicted) |
| Melting Point | 115-117°C |
| Boling Point | 153℃/23mm |
| Flash Point | 129.7°C |
| Solubility | DMSO (Slightly), Methanol (Slightly) |
| Vapor Presure | 0.00765mmHg at 25°C |
| Appearance | Crystalline powder |
| Color | Pink |
| pKa | 2.05±0.10(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
| Refractive Index | 1.558 |
| MDL | MFCD06200918 |
2-(Methoxycarbonyl)-6-methylaniline, 2-Amino-3-(methoxycarbonyl)toluene, Methyl 3-methylanthranilate - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S37/39 - Wear suitable gloves and eye/face protection |
| Hazard Class | IRRITANT |
2-(Methoxycarbonyl)-6-methylaniline, 2-Amino-3-(methoxycarbonyl)toluene, Methyl 3-methylanthranilate - Reference Information
| Introduction | Methyl 2-amino-3-methylbenzoate is an organic intermediate, which can be obtained by reducing nitro from methyl 3-methyl-2-nitrobenzoate as raw material or by reacting with methyl iodide. |
| preparation | methyl 3-methyl -2-nitrobenzoate (98.5g,505mmol), 5% Pd/C(Degussa CE105XRC/W,1.0g) and acetonitrile (300mL) are mixed in a 600-mL high pressure vessel. The mixture was heated to 70°C and hydrogenated at 65psi(450kPa) for 8h. Add another 5% Pd/C(1.0g) and continue hydrogenation at 100psi(690kPa) for 8.5h. After , cool the reaction mixture, purify with nitrogen, filter through Celite diatom filter aid, and wash with acetonitrile (3 × 25mL). The combined filtrate was partially evaporated to a weight of ~ 160g, and then diluted with acetonitrile to a total weight of 200g. |
Last Update：2024-04-09 21:01:54
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2-(Methoxycarbonyl)-6-methylaniline, 2-Amino-3-(methoxycarbonyl)toluene, Methyl 3-methylanthranilate